By Newton [Ed] Friend
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Extra resources for A textbook of inorganic chemistry vol.VII part III Chromium and its congeners
The techniques include time-lag focusing (or delayed extraction) [4, 7–10], the ion mirror (or reﬂectron) [11–13], impulse-ﬁeld focusing , velocity compaction , dynamic-ﬁeld focusing , and post-source pulse focusing . Of these, time-lag focusing and impulse-ﬁeld focusing are in-source techniques, whereas the others are post-source methods. Among these techniques, reﬂectron and time-lag focusing have been most widely used in MALDI–TOF mass spectrometers. 1 The Ion Mirror (Reﬂectron) As discussed above, the adjustments for the initial spatial distribution may be done in the source.
For more information on the topic of matrix selection, the reader is referred to the earlier chapters on sample preparation and to Chapter 6. 2 Cationization Agents The proper choice of the cationization agent is the key issue for MALDI of polymers. Polyethers are easily cationized by alkali metal ions; polymers containing aromatic moieties can be cationized with Ag+ or Cu+. In addition to these cations, which are by far the most widely used, a wide variety of salts have been employed for cationization of polymer samples .
Nucl. Instrum. Meth. Phys. Res. A, 2000, 444, 389. , Rapid Commun. , 2001, 15, 277. , J. , 2003, 38, 948. , Rapid Commun. , 1998, 12, 519. , 2002, 35, 7149. , J. Phys. Chem. A 2006, 110, 1426. , J. Am. Soc. Mass Spectrom. 2009, 20, 1327. , Appl. Spectrosc. Rev. 2008, 43, 485. , J. Phys. Chem. A, 2006, 110, 12728. , Proc. Natl. Acad. Sci. A. 2009, 106, 10092. , Int. J. Mass Spectrom. 2007, 268, 122. , J. Am. Soc. Mass Spectrom. 2009, 20, 1078. CH A P TE R 3 TIME-OF-FLIGHT MASS SPECTROMETRY FOR POLYMER CHARACTERIZATION Liang Li and Randy M.
A textbook of inorganic chemistry vol.VII part III Chromium and its congeners by Newton [Ed] Friend