By Hans Zimmer
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Extra info for Annual Reports in Inorganic and General Syntheses–1976
C ^ NH 2 (45%) J Z Et3N (40%) (fiJ J NH , 0 2 Si(NHSiMe^) 2 (70%), is obtained (89)· Stepwise substitution of 0 9 SiCl 9 may be achieved as reaction of 0 9 SiCl 9 and Et9NH provided jOi(CI)NEt (80%) (91)· Partial aminolysis of 0SiF with HNEt9 (1:2 ratio) l J gave 0SiF2NEt2 (55%) (92). Lithium salts of amines react with chlorosilanes to give silylamines. A 2:1 ratio (Me^iKNLi and SiCl4 gave (Me3Si)2NSiCl3 (86%) (89). Several studies of the reaction of lithium amides with silyl fluorides appeared and the types of products obtained include F 9 Si[N(Me)SiMeJ 9 (92), RSiF9[N(Bu )(SiMeJ] 9 (92), ^uSiFOiNBu*) [N(Buü) (SiMeJ] (93) and t B u ^ i W N H B u * ò l l J (94)· 96).
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A. G. A. V. Kisin and V . l . Pchelintsev, ZH. OBSHCH. , 45^,2221-3 (1975). A. G. A. M. Kuz'mina, ZH. OBSHCH. , 45^, 2223-6 (1975). M . E . Childs and W . P . Weber, J. ORG. , 4^, 1799-802 (1976). T. P. Gaspar, J. AM. CHEM. , 98^, 3715-16 (1976). J. Barton and M. , 3893-6 (1975). D. C. Annarelli, J. AM. CHEM. S O C , 97^, 7162-3 (1975). D. Seyferth, D . C Annarelli and S . C Vick, J. AM. CHEM. S O C , 98^, 6382-4 (1976). M. Ishikawa, T. Fuchikami and M. , 1299-302 (1976). C M . D. H. Sommer, J.
Annual Reports in Inorganic and General Syntheses–1976 by Hans Zimmer