Download e-book for iPad: Basics of Analytical Chemistry and Chemical Equilibria by Brian M. Tissue

By Brian M. Tissue

ISBN-10: 0470592087

ISBN-13: 9780470592083

ISBN-10: 1118647041

ISBN-13: 9781118647042

Content material:
Chapter 1 Making Measurements (pages 1–52):
Chapter 2 pattern instruction, Extractions, and Chromatography (pages 53–102):
Chapter three Classical equipment (pages 103–140):
Chapter four Molecular Spectroscopy (pages 141–175):
Chapter five Acid?Base Equilibria and task (pages 177–220):
Chapter 6 Buffer recommendations and Polyprotic Acids (pages 221–244):
Chapter 7 Complexation and Precipitation Equilibria (pages 245–291):
Chapter eight Electroanalytical Chemistry (pages 293–339):
Chapter nine Atomic Spectrometry (pages 340–366):
Chapter 10 Analytical Separations (pages 367–406):

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Extra info for Basics of Analytical Chemistry and Chemical Equilibria

Example text

Spectrophotometric grade: high purity solvent with very low absorbance in the UV spectral region. Manufacturers often have their own trademarked names for these grades. The purity required for a given application will often be specified in analytical procedures. Volumetric Glassware Maintaining the validity of high quality standards requires proper handling to avoid errors from contamination or reducing the accuracy of the concentration during weighing and solution preparation. The tools for accurate handling include the analytical balance, volumetric glassware, and proper laboratory techniques.

9 Glassware Calibration. 013 g of distilled water. 99777 g/ml. 99777 g/ml This calibration now gives us a more accurate value for this pipette. To be more certain of the value, we would repeat the calibration two or three times to get an average value. 10 Glassware Use. Calculate the relative error in delivering 98 and 8 ml of solution using a 100-ml graduated cylinder. The readability and thus the uncertainty of the graduated cylinder is ±1 ml. The uncertainty in delivering 98 ml is 98 ± 1 ml or 1 ml × 100% = 1% 98 ml The uncertainty in delivering 8 ml is 8 ± 1 ml or 1 ml × 100% = 12% 8 ml The uncertainty in delivering a volume is dependent on the relative amount of the liquid compared to the size of the glassware.

4 Source of a systematic error. for sample collection, preparation, and measurement that produce accurate and repeatable results. Very often this work has been done by someone else and you are using one or more standard methods. When a standard method is not available, analysts usually start with a method for a similar type of sample and modify it to obtain good results. Method validation is the process to ensure that you are obtaining accurate and repeatable results. 165 (e):25 The accuracy, sensitivity, specificity, and reproducibility of test methods employed by the firm shall be established and documented.

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Basics of Analytical Chemistry and Chemical Equilibria by Brian M. Tissue


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